1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE CAS 13754-86-4 is Intermediate of propranolol.
Shandong Believe Chemical Pte. Ltd.1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE CAS 13754-86-4production method:Resorcinol was hydrogenated and isomerized with nickel in the presence of potassium hydroxide to produce potassium 3-keto cyclohexyl-1-enol, which was then combined with ethyl bromopyruvate ring chemicalbook to obtain 4-oxo-4,5,6,7-tetrahydrocoumarone carboxylic Acid-3, and then ammonia was used to replace the oxygen on the furan ring of the latter and eliminate (decarboxylation) to obtain the product.
1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE CAS 13754-86-4
1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONEChemicalSpecification
Product Name |
1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE |
||
Formula |
C8H9NO |
Molecular Weight |
135.16 |
CAS NO. |
13754-86-4 |
Quantity |
500KG |
Items |
Specification |
|
Appearance |
Light yellow crystal |
|
Assay |
≥98% |
|
Melting point |
188-190 °C (lit.) |
|
Moisture |
≤0.5% |
|
结论 CONCLUSION |
The result conform with standard |
1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE CAS 13754-86-4
Synonym:4-Oxo-1,5,6,7-tetrahydroindole;1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE;1,5,6,7-TETRAHYDRO-4H-INDOLE-4-ONE;1,5,6,7-TETRAHYDRO-INDOLChemicalbook-4-ONE;4-OXO-4,5,6,7-TETRAHYDROINDOLE;Tetrahydroindolone;4-0xo-4,5,6,7-tetrahydroindole;1,5,6,7-TETRAHYDRO-4H-INDOL-4-ONE97+%
CAS: 13754-86-4
Molecular formula: C8H9NO
Molecular weight:135.16
Boiling point:311℃
Density:1.216
Storage conditions: 2-8°C
Flashing point:150
Refractive index:nD20 1.54032
Storage conditions:Store below +30°C.
Shelf life:2 years